Abstract

A comparative study is carried out on two spectroscopic techniques employed to detect ultrafast absorption changes in the mid-infrared spectral range, namely direct multichannel detection via HgCdTe (MCT) photodiode arrays and the newly established technique of chirped-pulse up-conversion (CPU). Whereas both methods are meanwhile individually used in a routine manner, we directly juxtapose their applicability in femtosecond pump-probe experiments based on 1 kHz shot-to-shot data acquisition. Additionally, we examine different phase-matching conditions in the CPU scheme for a given mid-infrared spectrum, thereby simultaneously detecting signals which are separated by more than 200 cm−1.

© 2013 Optical Society of America

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2013 (4)

P. Rudolf, F. Kanal, J. Knorr, C. Nagel, J. Niesel, T. Brixner, U. Schatzschneider, and P. Nuernberger, “Ultra-fast photochemistry of a manganese-tricarbonyl CO-releasing molecule (CORM) in aqueous solution,” J. Phys. Chem. Lett. 4, 596–602 (2013).
[Crossref]

Y. Nomura, Y.-T. Wang, T. Kozai, H. Shirai, A. Yabushita, C.-W. Luo, S. Nakanishi, and T. Fuji, “Single-shot detection of mid-infrared spectra by chirped-pulse upconversion with four-wave difference frequency generation in gases,” Opt. Express 21, 18249–18254 (2013).
[Crossref] [PubMed]

W. Rock, Y.-L. Li, P. Pagano, and C. M. Cheatum, “2D IR spectroscopy using four-wave mixing, pulse shaping, and IR upconversion: A quantitative comparison,” J. Phys. Chem. A 117, 6073–6083 (2013).
[Crossref] [PubMed]

M. Kaucikas, J. Barber, and J. J. van Thor, “Polarization sensitive ultrafast mid-IR pump probe micro-spectrometer with diffraction limited spatial resolution,” Opt. Express 21, 8357–8370 (2013).
[Crossref] [PubMed]

2012 (4)

J. Zhu, T. Mathes, A. D. Stahl, J. T. Kennis, and M. L. Groot, “Ultrafast mid-infrared spectroscopy by chirped pulse upconversion in 1800-1000 cm−1 region,” Opt. Express 20, 10562–10571 (2012).
[Crossref] [PubMed]

Y. Yang, M. Linke, T. von Haimberger, J. Hahn, R. Matute, L. González, P. Schmieder, and K. Heyne, “Real-time tracking of phytochrome’s orientational changes during Pr photoisomerization,” J. Am. Chem. Soc. 134, 1408–1411 (2012).
[Crossref] [PubMed]

J. P. Lomont, S. C. Nguyen, and C. B. Harris, “Ultrafast TRIR and DFT studies of the photochemical dynamics of Co4(CO)12in solution,” Organometallics 31, 4031–4038 (2012).
[Crossref]

A. Lukacs, R.-K. Zhao, A. Haigney, R. Brust, G. M. Greetham, M. Towrie, P. J. Tonge, and S. R. Meech, “Excited state structure and dynamics of the neutral and anionic flavin radical revealed by ultrafast transient mid-IR to visible spectroscopy,” J. Phys. Chem. B 116, 5810–5818 (2012).
[Crossref] [PubMed]

2011 (3)

S. Yan, M. T. Seidel, Z. Zhang, W. K. Leong, and H.-S. Tan, “Ultrafast vibrational relaxation dynamics of carbonyl stretching modes in Os3(CO)12,” J. Chem. Phys. 135, 024501 (2011).
[Crossref]

P. Nuernberger, K. F. Lee, A. Bonvalet, L. Bouzhir-Sima, J.-C. Lambry, U. Liebl, M. Joffre, and M. H. Vos, “Strong ligand-protein interactions revealed by ultrafast infrared spectroscopy of CO in the heme pocket of the oxygen sensor FixL,” J. Am. Chem. Soc. 133, 17110–17113 (2011).
[Crossref] [PubMed]

C. R. Baiz and K. J. Kubarych, “Ultrabroadband detection of a mid-IR continuum by chirped-pulse upconversion,” Opt. Lett. 36, 187–189 (2011).
[Crossref] [PubMed]

2010 (4)

P. Nuernberger, K. F. Lee, A. Bonvalet, M. H. Vos, and M. Joffre, “Multiply excited vibration of carbon monoxide in the primary docking site of hemoglobin following photolysis from the heme,” J. Phys. Chem. Lett. 1, 2077–2081 (2010).
[Crossref]

J. M. Anna, M. J. Nee, C. R. Baiz, R. McCanne, and K. J. Kubarych, “Measuring absorptive two-dimensional infrared spectra using chirped-pulse upconversion detection,” J. Opt. Soc. Am. B 27, 382–393 (2010).
[Crossref]

R. Maksimenka, P. Nuernberger, K. F. Lee, A. Bonvalet, J. Milkiewicz, C. Barta, M. Klima, T. Oksenhendler, P. Tournois, D. Kaplan, and M. Joffre, “Direct mid-infrared femtosecond pulse shaping with a calomel acousto-optic programmable dispersive filter,” Opt. Lett. 35, 3565–3567 (2010).
[Crossref] [PubMed]

P. Rudolf, J. Buback, J. Aulbach, P. Nuernberger, and T. Brixner, “Ultrafast multisequential photochemistry of 5-diazo Meldrum’s acid,” J. Am. Chem. Soc. 132, 15213–15222 (2010).
[Crossref] [PubMed]

2009 (2)

2008 (2)

Y. Zhang, G. Burdzinski, J. Kubicki, and M. S. Platz, “Direct observation of carbene and diazo formation from aryldiazirines by ultrafast infrared spectroscopy,” J. Am. Chem. Soc. 130, 16134–16135 (2008).
[Crossref] [PubMed]

N. Jacquinet-Husson, N.A. Scott, A. Chédin, L. Crépeau, R. Armante, V. Capelle, J. Orphal, A. Coustenis, C. Boonne, N. Poulet-Crovisier, A. Barbe, M. Birk, L.R. Brown, C. Camy-Peyret, C. Claveau, K. Chance, N. Christidis, C. Clerbaux, P.F. Coheur, V. Dana, L. Daumont, M.R. De Backer-Barilly, G. Di Lonardo, J.M. Flaud, A. Goldman, A. Hamdouni, M. Hess, M.D. Hurley, D. Jacquemart, I. Kleiner, P. Köpke, J.Y. Mandin, S. Massie, S. Mikhailenko, V. Nemtchinov, A. Nikitin, D. Newnham, A. Perrin, V.I. Perevalov, S. Pinnock, L. Régalia-Jarlot, C.P. Rinsland, A. Rublev, F. Schreier, L. Schult, K.M. Smith, S.A. Tashkun, J.L. Teffo, R.A. Toth, VI.G. Tyuterev, J. Vander Auwera, P. Varanasi, and G. Wagner, “The GEISA spectroscopic database: Current and future archive for earth and planetary atmosphere studies,” J. Quant. Spectrosc. Radiat. Transf. 109, 1043–1059 (2008).
[Crossref]

2007 (6)

M. J. Nee, R. McCanne, K. J. Kubarych, and M. Joffre, “Two-dimensional infrared spectroscopy detected by chirped pulse upconversion,” Opt. Lett. 32, 713–715 (2007).
[Crossref] [PubMed]

P. Nuernberger, G. Vogt, R. Selle, S. Fechner, T. Brixner, and G. Gerber, “Generation of shaped ultraviolet pulses at the third harmonic of titanium-sapphire femtosecond laser radiation,” Appl. Phys. B 88, 519–526 (2007).
[Crossref]

M. L. Groot, L. J. G. W. van Wilderen, and M. Di Donato, “Time-resolved methods in biophysics. 5. Femtosecond time-resolved and dispersed infrared spectroscopy on proteins,” Photochem. Photobiol. Sci. 6, 501–507 (2007).
[Crossref] [PubMed]

W. J. Schreier, T. E. Schrader, F. O. Koller, P. Gilch, C. E. Crespo-Hernández, V. N. Swaminathan, T. Carell, W. Zinth, and B. Kohler, “Thymine dimerization in DNA is an ultrafast photoreaction,” Science 315, 625–629 (2007).
[Crossref] [PubMed]

J. Treuffet, K. J. Kubarych, J.-C. Lambry, E. Pilet, J.-B. Masson, J.-L. Martin, M. H. Vos, M. Joffre, and A. Alexandrou, “Direct observation of ligand transfer and bond formation in cytochrome c oxidase by using mid-infrared chirped-pulse upconversion,” Proc. Natl. Acad. Sci. U.S.A 104, 15705–15710 (2007).
[Crossref] [PubMed]

D. Cringus, A. Bakulin, J. Lindner, P. Vöhringer, M. S. Pshenichnikov, and D. A. Wiersma, “Ultrafast energy transfer in water-AOT reverse micelles,” J. Phys. Chem. B 111, 14193–14207 (2007).
[Crossref] [PubMed]

2005 (2)

J. Bredenbeck, J. Helbing, J. R. Kumita, G. A. Woolley, and P. Hamm, “α-Helix formation in a photoswitchable peptide tracked from picoseconds to microseconds by time-resolved IR spectroscopy,” Proc. Natl. Acad. Sci. U.S.A. 102, 2379–2384 (2005).
[Crossref]

K. J. Kubarych, M. Joffre, A. Moore, N. Belabas, and D. M. Jonas, “Mid-infrared electric field characterization using a visible charge-coupled-device-based spectrometer,” Opt. Lett. 30, 1228–1230 (2005).
[Crossref] [PubMed]

2004 (1)

E. T. J. Nibbering and T. Elsaesser, “Ultrafast vibrational dynamics of hydrogen bonds in the condensed phase,” Chem. Rev. 104, 1887–1914 (2004).
[Crossref] [PubMed]

2003 (1)

G. Cerullo and S. D. Silvestri, “Ultrafast optical parametric amplifiers,” Rev. Sci. Instrum. 74, 1–18 (2003).
[Crossref]

2002 (2)

J. Herbst, K. Heyne, and R. Diller, “Femtosecond infrared spectroscopy of bacteriorhodopsin chromophore isomerization,” Science 297, 822–825 (2002).
[Crossref] [PubMed]

H. J. Bakker, H.-K. Nienhuys, G. Gallot, N. Lascoux, G. M. Gale, J.-C. Leicknam, and S. Bratos, “Transient absorption of vibrationally excited water,” J. Chem. Phys. 116, 2592–2598 (2002).
[Crossref]

2001 (1)

I. V. Rubtsov, T. Zhang, H. Nakajima, S. Aono, G. I. Rubtsov, S. Kumazaki, and K. Yoshihara, “Conformational dynamics of the transcriptional regulator CooA protein studied by subpicosecond mid-infrared vibrational spectroscopy,” J. Am. Chem. Soc. 123, 10056–10062 (2001).
[Crossref] [PubMed]

2000 (1)

1997 (1)

1995 (1)

M. Lim, T. Jackson, and P. Anfinrud, “Binding of CO to myoglobin from a heme pocket docking site to form nearly linear Fe-C-O,” Science 269, 962–966 (1995).
[Crossref] [PubMed]

1994 (2)

1992 (1)

P. Stoutland, R. Dyer, and W. Woodruff, “Ultrafast infrared spectroscopy,” Science 257, 1913–1917 (1992).
[Crossref] [PubMed]

1987 (1)

J. Moore, P. Hansen, and R. Hochstrasser, “A new method for picosecond time-resolved infrared spectroscopy: applications to CO photodissociation from iron porphyrins,” Chem. Phys. Letters 138, 110–114 (1987).
[Crossref]

Alexandrou, A.

J. Treuffet, K. J. Kubarych, J.-C. Lambry, E. Pilet, J.-B. Masson, J.-L. Martin, M. H. Vos, M. Joffre, and A. Alexandrou, “Direct observation of ligand transfer and bond formation in cytochrome c oxidase by using mid-infrared chirped-pulse upconversion,” Proc. Natl. Acad. Sci. U.S.A 104, 15705–15710 (2007).
[Crossref] [PubMed]

Anfinrud, P.

M. Lim, T. Jackson, and P. Anfinrud, “Binding of CO to myoglobin from a heme pocket docking site to form nearly linear Fe-C-O,” Science 269, 962–966 (1995).
[Crossref] [PubMed]

Anna, J. M.

Aono, S.

I. V. Rubtsov, T. Zhang, H. Nakajima, S. Aono, G. I. Rubtsov, S. Kumazaki, and K. Yoshihara, “Conformational dynamics of the transcriptional regulator CooA protein studied by subpicosecond mid-infrared vibrational spectroscopy,” J. Am. Chem. Soc. 123, 10056–10062 (2001).
[Crossref] [PubMed]

Armante, R.

N. Jacquinet-Husson, N.A. Scott, A. Chédin, L. Crépeau, R. Armante, V. Capelle, J. Orphal, A. Coustenis, C. Boonne, N. Poulet-Crovisier, A. Barbe, M. Birk, L.R. Brown, C. Camy-Peyret, C. Claveau, K. Chance, N. Christidis, C. Clerbaux, P.F. Coheur, V. Dana, L. Daumont, M.R. De Backer-Barilly, G. Di Lonardo, J.M. Flaud, A. Goldman, A. Hamdouni, M. Hess, M.D. Hurley, D. Jacquemart, I. Kleiner, P. Köpke, J.Y. Mandin, S. Massie, S. Mikhailenko, V. Nemtchinov, A. Nikitin, D. Newnham, A. Perrin, V.I. Perevalov, S. Pinnock, L. Régalia-Jarlot, C.P. Rinsland, A. Rublev, F. Schreier, L. Schult, K.M. Smith, S.A. Tashkun, J.L. Teffo, R.A. Toth, VI.G. Tyuterev, J. Vander Auwera, P. Varanasi, and G. Wagner, “The GEISA spectroscopic database: Current and future archive for earth and planetary atmosphere studies,” J. Quant. Spectrosc. Radiat. Transf. 109, 1043–1059 (2008).
[Crossref]

Aulbach, J.

P. Rudolf, J. Buback, J. Aulbach, P. Nuernberger, and T. Brixner, “Ultrafast multisequential photochemistry of 5-diazo Meldrum’s acid,” J. Am. Chem. Soc. 132, 15213–15222 (2010).
[Crossref] [PubMed]

Baiz, C. R.

Bakker, H. J.

H. J. Bakker, H.-K. Nienhuys, G. Gallot, N. Lascoux, G. M. Gale, J.-C. Leicknam, and S. Bratos, “Transient absorption of vibrationally excited water,” J. Chem. Phys. 116, 2592–2598 (2002).
[Crossref]

Bakulin, A.

D. Cringus, A. Bakulin, J. Lindner, P. Vöhringer, M. S. Pshenichnikov, and D. A. Wiersma, “Ultrafast energy transfer in water-AOT reverse micelles,” J. Phys. Chem. B 111, 14193–14207 (2007).
[Crossref] [PubMed]

Barbe, A.

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N. Jacquinet-Husson, N.A. Scott, A. Chédin, L. Crépeau, R. Armante, V. Capelle, J. Orphal, A. Coustenis, C. Boonne, N. Poulet-Crovisier, A. Barbe, M. Birk, L.R. Brown, C. Camy-Peyret, C. Claveau, K. Chance, N. Christidis, C. Clerbaux, P.F. Coheur, V. Dana, L. Daumont, M.R. De Backer-Barilly, G. Di Lonardo, J.M. Flaud, A. Goldman, A. Hamdouni, M. Hess, M.D. Hurley, D. Jacquemart, I. Kleiner, P. Köpke, J.Y. Mandin, S. Massie, S. Mikhailenko, V. Nemtchinov, A. Nikitin, D. Newnham, A. Perrin, V.I. Perevalov, S. Pinnock, L. Régalia-Jarlot, C.P. Rinsland, A. Rublev, F. Schreier, L. Schult, K.M. Smith, S.A. Tashkun, J.L. Teffo, R.A. Toth, VI.G. Tyuterev, J. Vander Auwera, P. Varanasi, and G. Wagner, “The GEISA spectroscopic database: Current and future archive for earth and planetary atmosphere studies,” J. Quant. Spectrosc. Radiat. Transf. 109, 1043–1059 (2008).
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Brixner, T.

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Buback, J.

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Burdzinski, G.

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Camy-Peyret, C.

N. Jacquinet-Husson, N.A. Scott, A. Chédin, L. Crépeau, R. Armante, V. Capelle, J. Orphal, A. Coustenis, C. Boonne, N. Poulet-Crovisier, A. Barbe, M. Birk, L.R. Brown, C. Camy-Peyret, C. Claveau, K. Chance, N. Christidis, C. Clerbaux, P.F. Coheur, V. Dana, L. Daumont, M.R. De Backer-Barilly, G. Di Lonardo, J.M. Flaud, A. Goldman, A. Hamdouni, M. Hess, M.D. Hurley, D. Jacquemart, I. Kleiner, P. Köpke, J.Y. Mandin, S. Massie, S. Mikhailenko, V. Nemtchinov, A. Nikitin, D. Newnham, A. Perrin, V.I. Perevalov, S. Pinnock, L. Régalia-Jarlot, C.P. Rinsland, A. Rublev, F. Schreier, L. Schult, K.M. Smith, S.A. Tashkun, J.L. Teffo, R.A. Toth, VI.G. Tyuterev, J. Vander Auwera, P. Varanasi, and G. Wagner, “The GEISA spectroscopic database: Current and future archive for earth and planetary atmosphere studies,” J. Quant. Spectrosc. Radiat. Transf. 109, 1043–1059 (2008).
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Capelle, V.

N. Jacquinet-Husson, N.A. Scott, A. Chédin, L. Crépeau, R. Armante, V. Capelle, J. Orphal, A. Coustenis, C. Boonne, N. Poulet-Crovisier, A. Barbe, M. Birk, L.R. Brown, C. Camy-Peyret, C. Claveau, K. Chance, N. Christidis, C. Clerbaux, P.F. Coheur, V. Dana, L. Daumont, M.R. De Backer-Barilly, G. Di Lonardo, J.M. Flaud, A. Goldman, A. Hamdouni, M. Hess, M.D. Hurley, D. Jacquemart, I. Kleiner, P. Köpke, J.Y. Mandin, S. Massie, S. Mikhailenko, V. Nemtchinov, A. Nikitin, D. Newnham, A. Perrin, V.I. Perevalov, S. Pinnock, L. Régalia-Jarlot, C.P. Rinsland, A. Rublev, F. Schreier, L. Schult, K.M. Smith, S.A. Tashkun, J.L. Teffo, R.A. Toth, VI.G. Tyuterev, J. Vander Auwera, P. Varanasi, and G. Wagner, “The GEISA spectroscopic database: Current and future archive for earth and planetary atmosphere studies,” J. Quant. Spectrosc. Radiat. Transf. 109, 1043–1059 (2008).
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Chance, K.

N. Jacquinet-Husson, N.A. Scott, A. Chédin, L. Crépeau, R. Armante, V. Capelle, J. Orphal, A. Coustenis, C. Boonne, N. Poulet-Crovisier, A. Barbe, M. Birk, L.R. Brown, C. Camy-Peyret, C. Claveau, K. Chance, N. Christidis, C. Clerbaux, P.F. Coheur, V. Dana, L. Daumont, M.R. De Backer-Barilly, G. Di Lonardo, J.M. Flaud, A. Goldman, A. Hamdouni, M. Hess, M.D. Hurley, D. Jacquemart, I. Kleiner, P. Köpke, J.Y. Mandin, S. Massie, S. Mikhailenko, V. Nemtchinov, A. Nikitin, D. Newnham, A. Perrin, V.I. Perevalov, S. Pinnock, L. Régalia-Jarlot, C.P. Rinsland, A. Rublev, F. Schreier, L. Schult, K.M. Smith, S.A. Tashkun, J.L. Teffo, R.A. Toth, VI.G. Tyuterev, J. Vander Auwera, P. Varanasi, and G. Wagner, “The GEISA spectroscopic database: Current and future archive for earth and planetary atmosphere studies,” J. Quant. Spectrosc. Radiat. Transf. 109, 1043–1059 (2008).
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Cheatum, C. M.

W. Rock, Y.-L. Li, P. Pagano, and C. M. Cheatum, “2D IR spectroscopy using four-wave mixing, pulse shaping, and IR upconversion: A quantitative comparison,” J. Phys. Chem. A 117, 6073–6083 (2013).
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Chédin, A.

N. Jacquinet-Husson, N.A. Scott, A. Chédin, L. Crépeau, R. Armante, V. Capelle, J. Orphal, A. Coustenis, C. Boonne, N. Poulet-Crovisier, A. Barbe, M. Birk, L.R. Brown, C. Camy-Peyret, C. Claveau, K. Chance, N. Christidis, C. Clerbaux, P.F. Coheur, V. Dana, L. Daumont, M.R. De Backer-Barilly, G. Di Lonardo, J.M. Flaud, A. Goldman, A. Hamdouni, M. Hess, M.D. Hurley, D. Jacquemart, I. Kleiner, P. Köpke, J.Y. Mandin, S. Massie, S. Mikhailenko, V. Nemtchinov, A. Nikitin, D. Newnham, A. Perrin, V.I. Perevalov, S. Pinnock, L. Régalia-Jarlot, C.P. Rinsland, A. Rublev, F. Schreier, L. Schult, K.M. Smith, S.A. Tashkun, J.L. Teffo, R.A. Toth, VI.G. Tyuterev, J. Vander Auwera, P. Varanasi, and G. Wagner, “The GEISA spectroscopic database: Current and future archive for earth and planetary atmosphere studies,” J. Quant. Spectrosc. Radiat. Transf. 109, 1043–1059 (2008).
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Christidis, N.

N. Jacquinet-Husson, N.A. Scott, A. Chédin, L. Crépeau, R. Armante, V. Capelle, J. Orphal, A. Coustenis, C. Boonne, N. Poulet-Crovisier, A. Barbe, M. Birk, L.R. Brown, C. Camy-Peyret, C. Claveau, K. Chance, N. Christidis, C. Clerbaux, P.F. Coheur, V. Dana, L. Daumont, M.R. De Backer-Barilly, G. Di Lonardo, J.M. Flaud, A. Goldman, A. Hamdouni, M. Hess, M.D. Hurley, D. Jacquemart, I. Kleiner, P. Köpke, J.Y. Mandin, S. Massie, S. Mikhailenko, V. Nemtchinov, A. Nikitin, D. Newnham, A. Perrin, V.I. Perevalov, S. Pinnock, L. Régalia-Jarlot, C.P. Rinsland, A. Rublev, F. Schreier, L. Schult, K.M. Smith, S.A. Tashkun, J.L. Teffo, R.A. Toth, VI.G. Tyuterev, J. Vander Auwera, P. Varanasi, and G. Wagner, “The GEISA spectroscopic database: Current and future archive for earth and planetary atmosphere studies,” J. Quant. Spectrosc. Radiat. Transf. 109, 1043–1059 (2008).
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Claveau, C.

N. Jacquinet-Husson, N.A. Scott, A. Chédin, L. Crépeau, R. Armante, V. Capelle, J. Orphal, A. Coustenis, C. Boonne, N. Poulet-Crovisier, A. Barbe, M. Birk, L.R. Brown, C. Camy-Peyret, C. Claveau, K. Chance, N. Christidis, C. Clerbaux, P.F. Coheur, V. Dana, L. Daumont, M.R. De Backer-Barilly, G. Di Lonardo, J.M. Flaud, A. Goldman, A. Hamdouni, M. Hess, M.D. Hurley, D. Jacquemart, I. Kleiner, P. Köpke, J.Y. Mandin, S. Massie, S. Mikhailenko, V. Nemtchinov, A. Nikitin, D. Newnham, A. Perrin, V.I. Perevalov, S. Pinnock, L. Régalia-Jarlot, C.P. Rinsland, A. Rublev, F. Schreier, L. Schult, K.M. Smith, S.A. Tashkun, J.L. Teffo, R.A. Toth, VI.G. Tyuterev, J. Vander Auwera, P. Varanasi, and G. Wagner, “The GEISA spectroscopic database: Current and future archive for earth and planetary atmosphere studies,” J. Quant. Spectrosc. Radiat. Transf. 109, 1043–1059 (2008).
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Clerbaux, C.

N. Jacquinet-Husson, N.A. Scott, A. Chédin, L. Crépeau, R. Armante, V. Capelle, J. Orphal, A. Coustenis, C. Boonne, N. Poulet-Crovisier, A. Barbe, M. Birk, L.R. Brown, C. Camy-Peyret, C. Claveau, K. Chance, N. Christidis, C. Clerbaux, P.F. Coheur, V. Dana, L. Daumont, M.R. De Backer-Barilly, G. Di Lonardo, J.M. Flaud, A. Goldman, A. Hamdouni, M. Hess, M.D. Hurley, D. Jacquemart, I. Kleiner, P. Köpke, J.Y. Mandin, S. Massie, S. Mikhailenko, V. Nemtchinov, A. Nikitin, D. Newnham, A. Perrin, V.I. Perevalov, S. Pinnock, L. Régalia-Jarlot, C.P. Rinsland, A. Rublev, F. Schreier, L. Schult, K.M. Smith, S.A. Tashkun, J.L. Teffo, R.A. Toth, VI.G. Tyuterev, J. Vander Auwera, P. Varanasi, and G. Wagner, “The GEISA spectroscopic database: Current and future archive for earth and planetary atmosphere studies,” J. Quant. Spectrosc. Radiat. Transf. 109, 1043–1059 (2008).
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Coheur, P.F.

N. Jacquinet-Husson, N.A. Scott, A. Chédin, L. Crépeau, R. Armante, V. Capelle, J. Orphal, A. Coustenis, C. Boonne, N. Poulet-Crovisier, A. Barbe, M. Birk, L.R. Brown, C. Camy-Peyret, C. Claveau, K. Chance, N. Christidis, C. Clerbaux, P.F. Coheur, V. Dana, L. Daumont, M.R. De Backer-Barilly, G. Di Lonardo, J.M. Flaud, A. Goldman, A. Hamdouni, M. Hess, M.D. Hurley, D. Jacquemart, I. Kleiner, P. Köpke, J.Y. Mandin, S. Massie, S. Mikhailenko, V. Nemtchinov, A. Nikitin, D. Newnham, A. Perrin, V.I. Perevalov, S. Pinnock, L. Régalia-Jarlot, C.P. Rinsland, A. Rublev, F. Schreier, L. Schult, K.M. Smith, S.A. Tashkun, J.L. Teffo, R.A. Toth, VI.G. Tyuterev, J. Vander Auwera, P. Varanasi, and G. Wagner, “The GEISA spectroscopic database: Current and future archive for earth and planetary atmosphere studies,” J. Quant. Spectrosc. Radiat. Transf. 109, 1043–1059 (2008).
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Coustenis, A.

N. Jacquinet-Husson, N.A. Scott, A. Chédin, L. Crépeau, R. Armante, V. Capelle, J. Orphal, A. Coustenis, C. Boonne, N. Poulet-Crovisier, A. Barbe, M. Birk, L.R. Brown, C. Camy-Peyret, C. Claveau, K. Chance, N. Christidis, C. Clerbaux, P.F. Coheur, V. Dana, L. Daumont, M.R. De Backer-Barilly, G. Di Lonardo, J.M. Flaud, A. Goldman, A. Hamdouni, M. Hess, M.D. Hurley, D. Jacquemart, I. Kleiner, P. Köpke, J.Y. Mandin, S. Massie, S. Mikhailenko, V. Nemtchinov, A. Nikitin, D. Newnham, A. Perrin, V.I. Perevalov, S. Pinnock, L. Régalia-Jarlot, C.P. Rinsland, A. Rublev, F. Schreier, L. Schult, K.M. Smith, S.A. Tashkun, J.L. Teffo, R.A. Toth, VI.G. Tyuterev, J. Vander Auwera, P. Varanasi, and G. Wagner, “The GEISA spectroscopic database: Current and future archive for earth and planetary atmosphere studies,” J. Quant. Spectrosc. Radiat. Transf. 109, 1043–1059 (2008).
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Crépeau, L.

N. Jacquinet-Husson, N.A. Scott, A. Chédin, L. Crépeau, R. Armante, V. Capelle, J. Orphal, A. Coustenis, C. Boonne, N. Poulet-Crovisier, A. Barbe, M. Birk, L.R. Brown, C. Camy-Peyret, C. Claveau, K. Chance, N. Christidis, C. Clerbaux, P.F. Coheur, V. Dana, L. Daumont, M.R. De Backer-Barilly, G. Di Lonardo, J.M. Flaud, A. Goldman, A. Hamdouni, M. Hess, M.D. Hurley, D. Jacquemart, I. Kleiner, P. Köpke, J.Y. Mandin, S. Massie, S. Mikhailenko, V. Nemtchinov, A. Nikitin, D. Newnham, A. Perrin, V.I. Perevalov, S. Pinnock, L. Régalia-Jarlot, C.P. Rinsland, A. Rublev, F. Schreier, L. Schult, K.M. Smith, S.A. Tashkun, J.L. Teffo, R.A. Toth, VI.G. Tyuterev, J. Vander Auwera, P. Varanasi, and G. Wagner, “The GEISA spectroscopic database: Current and future archive for earth and planetary atmosphere studies,” J. Quant. Spectrosc. Radiat. Transf. 109, 1043–1059 (2008).
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Crespo-Hernández, C. E.

W. J. Schreier, T. E. Schrader, F. O. Koller, P. Gilch, C. E. Crespo-Hernández, V. N. Swaminathan, T. Carell, W. Zinth, and B. Kohler, “Thymine dimerization in DNA is an ultrafast photoreaction,” Science 315, 625–629 (2007).
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Cringus, D.

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Dana, V.

N. Jacquinet-Husson, N.A. Scott, A. Chédin, L. Crépeau, R. Armante, V. Capelle, J. Orphal, A. Coustenis, C. Boonne, N. Poulet-Crovisier, A. Barbe, M. Birk, L.R. Brown, C. Camy-Peyret, C. Claveau, K. Chance, N. Christidis, C. Clerbaux, P.F. Coheur, V. Dana, L. Daumont, M.R. De Backer-Barilly, G. Di Lonardo, J.M. Flaud, A. Goldman, A. Hamdouni, M. Hess, M.D. Hurley, D. Jacquemart, I. Kleiner, P. Köpke, J.Y. Mandin, S. Massie, S. Mikhailenko, V. Nemtchinov, A. Nikitin, D. Newnham, A. Perrin, V.I. Perevalov, S. Pinnock, L. Régalia-Jarlot, C.P. Rinsland, A. Rublev, F. Schreier, L. Schult, K.M. Smith, S.A. Tashkun, J.L. Teffo, R.A. Toth, VI.G. Tyuterev, J. Vander Auwera, P. Varanasi, and G. Wagner, “The GEISA spectroscopic database: Current and future archive for earth and planetary atmosphere studies,” J. Quant. Spectrosc. Radiat. Transf. 109, 1043–1059 (2008).
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P. Rudolf, F. Kanal, J. Knorr, C. Nagel, J. Niesel, T. Brixner, U. Schatzschneider, and P. Nuernberger, “Ultra-fast photochemistry of a manganese-tricarbonyl CO-releasing molecule (CORM) in aqueous solution,” J. Phys. Chem. Lett. 4, 596–602 (2013).
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Nuernberger, P.

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K. F. Lee, P. Nuernberger, A. Bonvalet, and M. Joffre, “Removing cross-phase modulation from midinfrared chirped-pulse upconversion spectra,” Opt. Express 17, 18738–18744 (2009).
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Orphal, J.

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Perevalov, V.I.

N. Jacquinet-Husson, N.A. Scott, A. Chédin, L. Crépeau, R. Armante, V. Capelle, J. Orphal, A. Coustenis, C. Boonne, N. Poulet-Crovisier, A. Barbe, M. Birk, L.R. Brown, C. Camy-Peyret, C. Claveau, K. Chance, N. Christidis, C. Clerbaux, P.F. Coheur, V. Dana, L. Daumont, M.R. De Backer-Barilly, G. Di Lonardo, J.M. Flaud, A. Goldman, A. Hamdouni, M. Hess, M.D. Hurley, D. Jacquemart, I. Kleiner, P. Köpke, J.Y. Mandin, S. Massie, S. Mikhailenko, V. Nemtchinov, A. Nikitin, D. Newnham, A. Perrin, V.I. Perevalov, S. Pinnock, L. Régalia-Jarlot, C.P. Rinsland, A. Rublev, F. Schreier, L. Schult, K.M. Smith, S.A. Tashkun, J.L. Teffo, R.A. Toth, VI.G. Tyuterev, J. Vander Auwera, P. Varanasi, and G. Wagner, “The GEISA spectroscopic database: Current and future archive for earth and planetary atmosphere studies,” J. Quant. Spectrosc. Radiat. Transf. 109, 1043–1059 (2008).
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Perrin, A.

N. Jacquinet-Husson, N.A. Scott, A. Chédin, L. Crépeau, R. Armante, V. Capelle, J. Orphal, A. Coustenis, C. Boonne, N. Poulet-Crovisier, A. Barbe, M. Birk, L.R. Brown, C. Camy-Peyret, C. Claveau, K. Chance, N. Christidis, C. Clerbaux, P.F. Coheur, V. Dana, L. Daumont, M.R. De Backer-Barilly, G. Di Lonardo, J.M. Flaud, A. Goldman, A. Hamdouni, M. Hess, M.D. Hurley, D. Jacquemart, I. Kleiner, P. Köpke, J.Y. Mandin, S. Massie, S. Mikhailenko, V. Nemtchinov, A. Nikitin, D. Newnham, A. Perrin, V.I. Perevalov, S. Pinnock, L. Régalia-Jarlot, C.P. Rinsland, A. Rublev, F. Schreier, L. Schult, K.M. Smith, S.A. Tashkun, J.L. Teffo, R.A. Toth, VI.G. Tyuterev, J. Vander Auwera, P. Varanasi, and G. Wagner, “The GEISA spectroscopic database: Current and future archive for earth and planetary atmosphere studies,” J. Quant. Spectrosc. Radiat. Transf. 109, 1043–1059 (2008).
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Pilet, E.

J. Treuffet, K. J. Kubarych, J.-C. Lambry, E. Pilet, J.-B. Masson, J.-L. Martin, M. H. Vos, M. Joffre, and A. Alexandrou, “Direct observation of ligand transfer and bond formation in cytochrome c oxidase by using mid-infrared chirped-pulse upconversion,” Proc. Natl. Acad. Sci. U.S.A 104, 15705–15710 (2007).
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Figures (8)

Fig. 1
Fig. 1 Schematic illustration of the experimental setup: CPU, upconversion of MIR pulses via sum-frequency mixing with strongly chirped NIR pulses in a MgO:LiNbO3 crystal; F, 750 nm shortpass filter; BS, 50/50 MIR beam splitter; S, sample in flow cell; τ: translation stage to adjust the UV-pump/MIR-probe delay; C, mechanical chopper. Several mirrors and lenses are not sketched for clarity.

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Fig. 2
Fig. 2 MIR spectrum obtained with a single HgCdTe pixel by scanning the central IR spectrometer wavelength in steps of 1 nm (blue, centered at 2028 cm−1, FWHM 154 cm−1, 100 laser shots averaged per step, 5 min total measurement time); MIR spectrum after upconversion and chirp correction detected via CCD camera (red, centered at 14554 cm−1, FWHM 151 cm−1, 300 ms exposure time); the frequencies of the 16 most intense water vapor lines taken from the GEISA database [37] are depicted as gridlines.

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Fig. 3
Fig. 3 Transient absorption of Co4(CO)12 under 270 nm UV excitation: data is obtained via CPU (left) and multichannel MCT detection (right), respectively. For each time step 1000 pump-probe pairs are consecutively recorded with each detection method. No data interpolation was used in both graphics.

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Fig. 4
Fig. 4 Transient absorption spectrum of Co4(CO)12 at 6 ps pump-probe delay under 270 nm UV excitation: data obtained by averaging 25000 consecutive pump-probe pairs using CPU detection (red); the blue-shaded area illustrates the full detection range of direct MIR detection; the inset depicts the spectral increment of both detection methods: data points of direct MIR detection via MCT array (blue) are shown with 5 mOD vertical offset; vertical lines confine data points which are used for analysis of individual noise levels (confer Figs. 5 and 6).

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Fig. 5
Fig. 5 Histograms illustrating the distribution of 50000 consecutively measured pump-probe pairs for the detection of the signal baseline (top row, no sample) and the detection of a molecular signal of ΔAbs ≈ 2 mOD at 2039 cm−1 (bottom row, sample and pump-interaction). Besides the histograms for CPU detection (left panels, red) and MCT detection (right panels, blue), representing a single data point, the results for an additional binning of five adjacent CPU data points are shown (middle panels, green). Distributions resulting after normalization of individual spectra with their integrated spectral intensity are shown for CPU detection (left panels, black) and CPU detection with an additional binning of five adjacent data points (middle panels, gray).

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Fig. 6
Fig. 6 Absorption-change noise level of a single data point at 2039 cm−1 when detecting ΔAbs = 0 (left panel, no sample) and ΔAbs ≈ 2 mOD (right panel, sample and pump-interaction): standard error versus the number of considered background-corrected pump-probe pairs using MCT detection (blue), CPU (red) or CPU with an additional binning of five adjacent data points (green). Noise levels resulting after normalization of individual spectra with their integrated spectral intensity are shown for CPU detection (black) and CPU detection with an additional binning of five adjacent data points (gray). Note that these graphs have a double-logarithmic scale.

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Fig. 7
Fig. 7 Absorption-change standard error as a function of the spectral position: data obtained via MCT (blue) and CPU detection (red) after averaging 25000 consecutive pump-probe pairs when detecting ΔAbs = 0 (solid lines, no sample) and a molecular signal (dashed lines, sample and pump-interaction, confer transient absorption spectra in Fig. 4); the CPU curves with binned data points or with normalized spectra, or with both, are not shown for clarity; the corresponding CPU spectra, with sample (light red) and without sample (light gray), are shown in the background.

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Fig. 8
Fig. 8 (a) MIR spectrum obtained with a single MCT pixel by scanning the central IR spectrometer wavelength in steps of 1 nm (centered at 1940 cm−1, FWHM 185 cm−1, 100 laser shots averaged per step). (b) MIR absorption spectrum of Co4(CO)12 dissolved in CH2Cl2. (c) Measured CPU spectra at different phase-matching angles. (d) Simulated CPU spectra at different phase-matching angles. (e) Transient absorption spectra of Co4(CO)12 at 6 ps pump-probe delay: data obtained by averaging 100000 consecutive pump-probe pairs at CPU phase-matching angles of θ = 45.5° (red) and θ = 44.5° (cyan, 10 mOD vertical offset).

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Tables (1)

Tables Icon

Table 1 Standard deviation of 50000 consecutively measured pump-probe pairs at 2039 cm−1 corresponding to the histograms shown in Fig. 5.

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Equations (2)

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Δ k = k NIR + k MIR − k SFG ,
I SFG = 8 d eff 2 ω SFG 2 I NIR I MIR n NIR n MIR n SFG ε 0 c 2 L 2 sin c 2 ( Δ k L 2 ) ,

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